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N-Dodecyltrichlorosilane

Meisheng Chemical

N-Dodecyltrichlorosilane
Specifications

HS Code

452587

Chemical Formula C12H25Cl3Si
Molecular Weight 307.77
Appearance Colorless to pale yellow liquid
Boiling Point ~295 - 300 °C
Density ~1.04 g/cm³
Solubility Reacts with water, soluble in most organic solvents
Vapor Pressure Low at room temperature
Flash Point ~110 °C
Refractive Index ~1.452
Packing & Storage
Packing N - Dodecyltrichlorosilane in 500 - ml bottles, well - sealed for safe storage.
Storage N - Dodecyltrichlorosilane should be stored in a cool, dry, well - ventilated area, away from heat sources and direct sunlight. Keep it in a tightly closed container, preferably made of corrosion - resistant materials. Store it separately from water, moisture, and reactive substances like bases, as it reacts vigorously with them. Ensure proper labeling for easy identification and safety.
Shipping N - Dodecyltrichlorosilane is a chemical. It should be shipped in sealed, corrosion - resistant containers. Ensure proper labeling indicating its hazardous nature. Ship via carriers compliant with chemical transportation regulations to prevent spills and ensure safety.
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N-Dodecyltrichlorosilane
General Information
Historical Development
N - Dodecyltrichlorosilane, the organosilicon compound is also. It is increasingly important in the field of chemical materials. Looking back to the past, the initial understanding of it was still shallow, and only a little bit of its basic properties were known. However, with the evolution of scientific research, scholars have carefully studied it, and discovered its unique reaction mechanism and wide application. In the past, the preparation of this compound was quite difficult, the yield was not high and the purity was not good. However, scientific researchers have made unremitting efforts to explore, improve the process, and make the preparation method more and more perfect. Today, N - Dodecyltrichlorosilane is useful in surface treatment, material modification and other fields, and has made great contributions to the development of many industries. Its historical evolution is a witness to the progress of scientific research, paving the way for more innovation in the future.
Product Overview
There is a substance today, named N-Dodecyltrichlorosilane. Its shape is a colorless, transparent to yellowish liquid, with a stimulating breath. This substance is widely used in the chemical industry. It is active, reacts when exposed to water, and produces hydrogen chloride gas. It can be used as a coupling agent to closely connect inorganic and organic substances to strengthen material properties. It can also be a surface treatment agent to form a film on the surface of the material to increase its hydrophobicity and wear resistance. When preparing, the reaction conditions need to be controlled to ensure the purity of the product. When using, pay attention to safety, because it is corrosive and irritating. The operation should be in a well-ventilated place, wearing protective equipment to avoid contact with the skin and eyes. This is the N - Dodecyltrichlorosilane general situation and use.
Physical & Chemical Properties
N - Dodecyltrichlorosilane, silicone compounds are also. Its physical and chemical properties are unique and important. Looking at its physical properties, it is a colorless to light yellow liquid at room temperature, with a pungent odor. Its boiling point is considerable, because of the intermolecular force. As for solubility, it can be soluble in many organic solvents, such as toluene, ether and the like. In terms of its chemical properties, the activity is quite high. Because it contains trichlorosilane groups, it is easy to hydrolyze and reacts in contact with water to form silanol and hydrogen chloride. This hydrolysis reaction is very fast. In the field of organic synthesis, it can be used as a silane coupling agent to build a stable connection between organic and inorganic substances. Its long chain dodecyl group gives the material hydrophobicity. In the field of material surface modification, it is widely used to improve the physical and chemical properties of materials, increase their durability and stability.
Technical Specifications & Labeling
Today there are N - Dodecyltrichlorosilane this material, which is widely used in industry and scientific research. Its technical specifications and identification (product parameters) are the key. In terms of technical specifications, its purity must reach a very high standard, and the impurity content must be strictly controlled. In terms of physical properties, such as color and morphology, etc., its boiling point and melting point must also be accurately controlled to meet the needs of the application. As for the label, on the product label, the name, chemical formula and other basic information should be clear. Warning labels are indispensable to inform users of latent risks. Batch, production date, etc. should also be recorded in detail for traceability. In this way, it can ensure its quality and safety during production and use, so that it can perform its functions.
Preparation Method
The method of making N-Dodecyltrichlorosilane is related to the raw materials and production process, reaction steps and catalytic mechanism. The raw materials are often taken from dodecanol and trichlorosilane. First prepare a clean and dry reactor, and add dodecanol and trichlorosilane into the kettle according to a specific ratio. The reaction is in an inert gas atmosphere, and the temperature is controlled appropriately, such as between 40 and 60 degrees Celsius. Metal halide is used as a catalyst to promote the reaction. At the beginning of the reaction, the two slowly combine and go through stirring, condensation and other steps. During this period, the reaction process is closely monitored to observe the temperature and pressure changes. After the reaction is completed, the impurities are removed by distillation and purification to obtain a pure N-Dodecyltrichlorosilane product. In this way, a good method for preparing this chemical can be obtained.
Chemical Reactions & Modifications
Recently, in the field of chemistry, it is quite beneficial to study the reaction and modification of N-Dodecyltrichlorosilane this substance. Its chemical properties are very active, and it often changes strangely when it comes into contact with other substances. Looking at its reaction, in a suitable environment, it can meet with water and hydrolyze, chlorine leaves, and becomes a genus of silanol. This change can lead to subsequent reactions to build new structures. It can also meet with alcohols, and it should be hydrolyzed. When changing its group, its chemical properties also vary. When talking about modification, based on it, adding other functional groups can change its appearance and increase its affinity. Or it can be combined with the polymer, fused in it, and the quality of the material can be strengthened, so that it can be used in industry and scientific research. These reactions and modifications are the road to chemical research, expanding the path, and expecting more ingenious gains in the future to be used by the world.
Synonyms & Product Names
N - Dodecyltrichlorosilane, this substance is also known as dodecyl trichlorosilane. Looking at its name, "N - Dodecyl" means dodecyl, and "trichlorosilane" means trichlorosilane, and the combination of the two is the name of the compound. In the industry, there may be another name. In the field of chemical industry, the same substance has different names due to different regions, habits, and process focuses. However, no matter what it is called, it refers to this substance. In many chemical classics and practice records, although there are occasional nicknames, its chemical essence is constant. When we explore this substance, we should focus on its chemical properties and reaction mechanism, and the name changes. However, the appearance and the internal quality are the right way to study the chemical industry.
Safety & Operational Standards
"Specifications for the safety and operation of N-dodecyl trichlorosilane" For N-dodecyl trichlorosilane, it is also a chemical substance. It is active, and when operating, it is necessary to abide by safety and operating standards to ensure safety. In terms of safety, this substance is corrosive, and it can cause injury when it touches the skin and enters the eyes. Therefore, the operator must wear protective equipment, such as corrosion-resistant clothing, protective glasses, gloves, etc., to prevent accidental contact. If the skin touches occasionally, rinse quickly with a lot of water, followed by appropriate medicine; if it enters the eyes, it is especially necessary to rinse immediately and seek medical attention urgently. In addition, it is easy to hydrolyze in the air, generating hydrogen chloride gas, which is pungent and harmful. In the place of operation, when the ventilation is good, or a ventilation device is provided to prevent the accumulation of toxic gases. As for the operating specifications, when taking it, it should be in the fume hood to avoid harmful gases from being scattered. The weighing device must be accurate, and the dosage should be taken as needed, so as not to waste it. When dissolving or reacting, it must be added slowly and stirred evenly to prevent overreaction. The temperature and time of the reaction must be in accordance with the established laws and must not be changed without authorization. After use, store it properly, and place it in a dry and cool place to avoid contact with water and moisture. All of these are the main principles for the safety and operation of N-dodecyl trichlorosilane. From this, the operation can be guaranteed smoothly and the danger can be avoided.
Application Area
N-dodecyl trichlorosilane is widely used in industry. It plays an important role in the surface modification of materials. By treating the surface of the material, it can give it hydrophobicity. Such as building materials, treated with this substance, it can resist water and moisture, prolong its service life. In the field of electronics, it also has its uses. It can help the manufacture of semiconductor devices, improve their interface characteristics, and enhance the performance of electronic components. Furthermore, in the textile industry, the application of this substance can give fabrics special properties, such as waterproof, anti-fouling, etc., and improve the quality of fabrics. It has unique effects in various application fields, and is actually an important chemical substance.
Research & Development
In modern times, chemistry has flourished, and the research on the properties and uses of various things has deepened. I focus on the research of N-Dodecyltrichlorosilane. Its unique nature, wide range of uses, and great potential in the field of material surface modification. I initially investigated its physical and chemical properties, and tested its reaction rules in detail. I also explored its preparation methods, and strived to optimize the process, reduce its cost and increase its yield. There are many difficulties during the period, but I am determined. Today, it has been slightly effective, the preparation method is gradually improving, and the product quality has also improved. However, there is no end to learning. In the future, we should continue to study and expand its application field, hoping to benefit the industry and people's livelihood. We will do our best to make this research result widely beneficial to the world and promote the progress and development of the chemical field.
Toxicity Research
Since modern times, the toxicity of chemical substances has become more and more important. Now look at N-Dodecyltrichlorosilane, the toxicity of this substance, related to people's livelihood and scientific research. At the beginning, test its impact on organisms. Take insects, plants and trees to test, and observe its vitality changes. Insects touch it, or the action is stagnant, or even die; grass dips into its liquid, leaves gradually wilt, and vitality fades. Re-explore its role in the environment. If it flows in water and soil, those with clear water become turbid, those with fertile soil become barren, and biological chains are disturbed by it. Therefore, the toxicity of studying N-Dodecyltrichlorosilane should not be ignored. It is necessary to investigate carefully and clarify the harm, so as to prevent the trouble from unfolding and ensure the safety of all things.
Future Prospects
There is a thing today, named N-Dodecyltrichlorosilane, which has extraordinary hope in our chemical research. This material has special properties and has a wide range of uses. It can be applied to the surface modification of materials to make the material specific, waterproof, wear-resistant and other functions can be sought. Looking at its future, it can show its skills in the field of high-tech materials. Electronic device manufacturing, hoping that its material performance will soar, making the chip better and running smoother. And in aerospace, or it can help the aircraft shell is light and strong, resistant to corrosion and wear, and resistant to the harsh environment of space. Furthermore, in biomedicine, it can also be used. Or it can modify biological materials, promote cell adhesion and proliferation, and add new power to tissue engineering. We should study it diligently, explore its endless potential, and hope to use this thing in the future to open a new chapter in technology and create well-being for the world.
Frequently Asked Questions
What are the main uses of N-Dodecyltrichlorosilane?
N-dodecyl trichlorosilane is also an organosilicon compound. It has a wide range of uses and is used in various fields of chemical industry. The first to bear the brunt is in the field of material surface modification. Applying it to the surface of the material can change the surface properties. If the surface of the material is hydrophobic, this is because the dodecyl group is a hydrophobic group. After its treatment, the contact angle of water on the surface of the material increases, and the water is difficult to infiltrate. It is very useful for waterproof materials, such as building waterproof coatings and fabric waterproof finishing. Taking fabric waterproof finishing as an example, after being treated with N-dodecyl trichlorosilane, the fabric can resist water without losing its breathability, which is suitable for outdoor clothing. Furthermore, it is also an important raw material when preparing silicone polymers. Polymerization with other compounds can produce polymers with specific properties. Such polymers may have good heat and weather resistance, and are often used in materials in high temperature environments, such as materials used in some components in the aerospace field. With the characteristics of this polymer, it can resist high temperature and severe weather erosion. In the coating industry, N-dodecyl trichlorosilane is also indispensable. Adding to the coating can improve the adhesion between the coating and the substrate, make the coating adhere more firmly to the surface of the object, and improve the wear resistance and chemical corrosion resistance of the coating. In this way, the service life of the coating is extended, and it can better protect the coated object and maintain its appearance and performance in the construction, automotive painting and other industries. In addition, in the field of electronics, it can be used for surface treatment of semiconductor materials. Improve the electrical properties and chemical stability of the surface of semiconductor materials, ensure the stable operation of electronic components, and ensure the performance of components in integrated circuits and other manufacturing processes.
What are the physical properties of N-Dodecyltrichlorosilane?
N-dodecyl trichlorosilane is also an organosilicon compound. It has various physical properties. Looking at its properties, it is a colorless to light yellow transparent liquid under normal conditions, and this color state is easy to detect. When it comes to density, it is about 0.99-1.03g/cm ³. The weight can be obtained by the quantity, and its floating and sinking state is known when mixing. In terms of boiling point, it is roughly between 295-305 ° C. When heated to this temperature, the liquid will dissolve gas. This boiling point is a key parameter for the separation and purification of this compound. The melting point is about -30 ° C. When cooled to this temperature, the liquid can solidify. Its solubility is also an important property. It is soluble in organic solvents such as toluene and xylene, but rapidly hydrolyzes in water to produce corresponding silanol and hydrochloric acid. This hydrolysis must be careful when applying, because the hydrolysis product may affect the reaction process and product purity. In addition, N-dodecyl trichlorosilane is volatile. Although the volatilization rate is not extremely fast, it gradually disperses in the air in the exposed environment. When storing and using this volatility, it should be carefully sealed to prevent the loss of its dissipation, and because it may be irritating, the dissipation is also harmful to the surrounding environment and human health.
N-Dodecyltrichlorosilane what are the precautions during use
N-dodecyl trichlorosilane is an organosilicon compound, and there are many points to be paid attention to during use. First safety protection. This compound is corrosive and can cause damage if it touches the skin, eyes, or is inhaled or ingested. Users must wear appropriate protective equipment, such as protective gloves, goggles, gas masks, etc., to avoid direct contact. In case of inadvertent contact, rinse with plenty of water immediately and seek medical attention in time. This is secondary to environmental factors. Because it is easy to hydrolyze in contact with water and generate acidic substances such as hydrogen chloride, it should be stored and used in a dry environment to avoid contact with water sources. And operate in a well-ventilated place to prevent the accumulation of harmful gases generated. After the operation, properly dispose of the waste and do not discard it at will, so as not to pollute the environment. Furthermore, it is related to the reaction conditions. When using, the reaction temperature, humidity and the ratio of reactants should be strictly controlled. Its hydrolysis reaction is rapid. In organic synthesis, it is necessary to follow the specific reaction requirements, or create anhydrous conditions, or make reasonable use of its hydrolysis characteristics to achieve the desired reaction effect. In addition, in terms of storage, it should be stored in a cool, dry and well-ventilated place, away from fire and heat sources, and stored separately from oxidants, acids, alkalis, etc., and should not be mixed. Regularly check whether the storage container is in good condition to prevent leakage. In conclusion, when using N-dodecyl trichlorosilane, careful attention should be paid to safety, environment, reaction conditions, and storage to ensure smooth operation and personnel and environmental safety.
Is N-Dodecyltrichlorosilane chemically stable?
N - dodecyl trichlorosilane, its chemical properties are relatively stable at room temperature and pressure. This substance contains trichlorosilyl and dodecyl. Trichlorosilyl has high activity and reacts violently in contact with water. Hydrolysis produces silicic acid and hydrogen chloride gas: \ [\ text {R} -\ text {SiCl} _ {3} + 3\ text {H} _ {2}\ text {O}\ rightarrow\ text {R} -\ text {Si (OH) } _ {3} + 3\ text {HCl}\ uparrow\] where\ (\ text {R}\) is dodecyl. Hydrogen chloride is irritating and escapes in the air to form an acid mist. The silicic acid formed by hydrolysis may be condensed and polymerized to synthesize polysiloxane. Dodecyl is a long-chain alkyl group with lipophilic properties, which makes the substance soluble in organic solvents, such as hydrocarbons, halogenated hydrocarbons, etc. However, its chemical stability is also affected by factors such as temperature, humidity, and contact substances. At high temperatures, its reactivity may increase, accelerating hydrolysis and other chemical reactions. In contact with alcohols, trichlorosilane can be substituted with alcohol hydroxyl groups to form silicon ethers: \ [\ text {R} -\ text {SiCl} _ {3} + 3\ text {R} '\ text {OH}\ rightarrow\ text {R} -\ text {Si (OR') } _ {3} + 3\ text {HCl}\] where,\ (\ text {R} '\) is an alkyl group in an alcohol. And N-dodecyl trichlorosilane can react with compounds containing active hydrogen, such as amines and carboxylic acids. When reacting with amines, chlorine atoms in trichlorosilane groups can be replaced by amine groups. When storing, it should be placed in a dry, cool and well-ventilated place to prevent hydrolysis and deterioration caused by water vapor intrusion. Due to the above chemical properties, N-dodecyl trichlorosilane is often used as a raw material for the synthesis of silicone compounds and a surface treatment agent, and is widely used in many fields of chemical industry.
What is N-Dodecyltrichlorosilane synthesis method?
The synthesis of N-dodecyl trichlorosilane is a key technique in chemical preparation. The process usually begins with the reaction of dodecyl halide and silica powder. In a suitable reactor, silica powder is placed and pretreated to make its activity suitable. Then, the dodecyl halide, such as dodecyl chloride, is slowly injected. This process requires precise temperature control and is generally maintained at a specific temperature range. This range varies depending on the catalyst used and the reaction conditions, roughly between 150 and 300 degrees Celsius. To promote the efficient progress of the reaction, a specific catalyst is often required. For example, copper-based catalysts can significantly reduce the activation energy of the reaction and accelerate the reaction rate. In the reaction, it is necessary to continue stirring to ensure that the reactants are fully contacted and the reaction proceeds uniformly. After the reaction is completed, the product contains N-dodecyl trichlorosilane and unreacted raw materials and by-products. At this time, a series of separation and purification steps are required. First, the crude product of the target product is initially separated by distillation according to the difference in the boiling point of each component. Then, by extraction, a suitable organic solvent is selected to further remove impurities and improve the purity of the product. Finally, high-purity N-dodecyl trichlorosilane can be obtained by distillation. This synthesis method requires fine control of each link condition in order to obtain the ideal yield and purity, which is of great significance in the preparation of silicone materials and other fields.